Thesis Abstract

Abstract
Metal-organic frameworks (MOFs) have garnered significant attention in recent years due to their unique properties and potential applications in gas adsorption. This thesis presents a comprehensive study on the synthesis and characterization of novel MOFs for gas adsorption applications. The research aims to explore the feasibility of utilizing these materials for efficient gas storage and separation. Through a combination of experimental synthesis techniques and advanced characterization methods, the properties of the synthesized MOFs were assessed to determine their potential for gas adsorption. Chapter one provides an introduction to the research topic, highlighting the background of the study, problem statement, objectives, limitations, scope, significance, and structure of the thesis. The chapter also defines key terms relevant to the study to provide a clear understanding of the research focus. Chapter two presents a thorough literature review covering ten key aspects related to MOFs, gas adsorption, synthesis methods, characterization techniques, and previous studies on similar materials. This review sets the stage for the subsequent chapters by establishing the current state of knowledge in the field and identifying gaps that this research aims to address. Chapter three details the research methodology employed in this study, including the synthesis protocols for producing the novel MOFs, the characterization techniques utilized to analyze their structural and adsorption properties, and the experimental procedures for evaluating gas adsorption performance. The chapter outlines the steps taken to ensure the reliability and reproducibility of the results obtained. In chapter four, the findings from the experimental investigations are comprehensively discussed, focusing on the structural features, surface properties, and gas adsorption capacities of the synthesized MOFs. The results are analyzed in depth to elucidate the relationship between the material structure and its gas adsorption performance, providing insights into the potential applications of these novel MOFs in gas storage and separation processes. Chapter five concludes the thesis by summarizing the key findings, discussing the implications of the research outcomes, and suggesting future directions for further studies in this field. The conclusions drawn from the study contribute to a better understanding of the synthesis and characterization of MOFs for gas adsorption applications, paving the way for the development of advanced materials with enhanced gas storage and separation capabilities. Overall, this thesis presents a systematic investigation into the synthesis and characterization of novel MOFs for gas adsorption applications, offering valuable insights into the potential of these materials in addressing challenges related to gas storage and separation. The findings contribute to the growing body of knowledge on MOFs and lay the foundation for future research endeavors in this exciting and rapidly evolving field.

Thesis Overview

The project titled "Synthesis and Characterization of Novel Metal-Organic Frameworks for Gas Adsorption Applications" aims to explore the synthesis, characterization, and potential applications of novel metal-organic frameworks (MOFs) in gas adsorption. MOFs are a class of porous materials composed of metal ions or clusters linked by organic ligands, offering a high surface area and tunable properties that make them promising candidates for gas storage and separation applications. The research will begin with a comprehensive literature review to provide a background on MOFs, their synthesis methods, characterization techniques, and previous studies on gas adsorption using MOFs. This review will highlight the recent advancements in the field and identify gaps in knowledge that the current study aims to address. The synthesis of novel MOFs will be a key focus of this research, with an emphasis on designing structures with tailored properties for enhanced gas adsorption performance. Various synthetic strategies will be explored, including solvothermal and microwave-assisted methods, to produce MOFs with specific pore sizes, surface chemistries, and thermal stabilities. Characterization techniques such as X-ray diffraction, scanning electron microscopy, gas adsorption measurements, and thermal analysis will be employed to study the structural, morphological, and gas adsorption properties of the synthesized MOFs. These analyses will provide insights into the pore structure, surface area, and gas sorption behavior of the materials, which are crucial for understanding their potential applications in gas storage and separation. The gas adsorption performance of the novel MOFs will be evaluated using different gases of industrial relevance, such as methane, carbon dioxide, and hydrogen. The adsorption capacities, selectivity, and kinetics of the MOFs will be investigated to assess their suitability for various gas storage and separation applications, including carbon capture and storage, natural gas purification, and hydrogen storage. Overall, this research aims to contribute to the development of advanced MOF materials with optimized properties for efficient gas adsorption applications. The findings from this study have the potential to enhance our understanding of MOF-based gas adsorbents and pave the way for their practical implementation in addressing key environmental and energy challenges.